International Journal of Education & Applied Sciences Research

International Journal of Education & Applied Sciences Research

Print ISSN : 2349 –4808

Online ISSN : 2349 –2899

Frequency : Continuous

Current Issue : Volume 2 , Issue 9
2015

SYNTHESIS MORPHOLOGY AND STRUCTURAL CHARACTERIZATION OF ZINC FERRITE NANOPARTICLES

V. D. Murumkar

Department of Physics, Vivekanand Arts, Sardar Dalipsingh Commerce and Science College, Aurangabad, Maharashtra State, India

DOI : Page No : 51-58

Published Online : 2015-10-30

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Abstract

Zinc ferrite (ZnFe2O4) nanoparticles were synthesized by sol-gel auto combustion method using citric acid as a fuel. The metal nitrate to fuel ratio was taken as 1:3. The as synthesized powder of Zn ferrite nanoparticles is annealed at 600˚C for 6 h and prepared sample was used for characterization and investigations of structural and magnetic properties. The structural characterization of Zn ferrite nanoparticles were done by X-ray diffraction technique. The crystallite size obtained by Scherer’s formula is in the order of 29 nm. The lattice constant determined from XRD data is in the reported range 8.429 Å. The morphological properties were investigated using scanning electron microscopy.

 

Keywords: Zn ferrite, Sol-gel auto-combustion, XRD, SEM, Garnet

Int. J. of Edu. & App. Sci. Research